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Arizona Administrative Code (Last Updated: November 17, 2016) |
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Title 3. AGRICULTURE |
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Chapter 3. DEPARTMENT OF AGRICULTURE ENVIRONMENTAL SERVICES DIVISION |
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Article 7. PESTICIDE |
Section R3-3-704. Labels
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A. Within two weeks of a pesticide label revision, a registrant shall provide the Department with two pesticide labels that have been revised since the pesticide was originally registered.
B. The Associate Director may request a copy of a pesticide label if the label on file is older than three years.
ALLOWED DEVIATIONS OF ANALYTICAL RESULTS FROM LABEL CLAIMS FOR ACTIVE INGREDIENTS IN PESTICIDE FORMULATIONS
Claim
%
HCV(1)
%
HSD(2)
Allowed Deviations for “uniform”(3) samples
Allowed Deviations for “non-uniform”(4) samples
Claim
- 3HSD
Claim
+ 6HSD
Claim
- 4HSD
Claim
+ 8HSD
0.001
11.31
0.00011
0.00066
0.00168
0.00055
0.00191
0.005
8.88
0.00044
0.0037
0.0077
0.0032
0.0086
0.008
8.27
0.00066
0.0060
0.0120
0.0054
0.0133
0.01
8.00
0.00080
0.0076
0.0148
0.0068
0.0164
0.03
6.78
0.0020
0.024
0.042
0.022
0.046
0.06
6.11
0.0037
0.049
0.082
0.045
0.089
0.10
5.66
0.0057
0.083
0.13
0.077
0.145
0.40
4.59
0.018
0.34
0.51
0.33
0.55
0.80
4.14
0.033
0.70
1.00
0.67
1.06
1.0
4.00
0.040
0.88
1.24
0.84
1.32
2.0
3.60
0.072
1.78
2.43
1.71
2.58
4.0
3.25
0.13
3.61
4.78
3.48
5.04
6.0
3.05
0.18
5.45
7.10
5.27
7.47
10.0
2.83
0.28
9.15
11.70
8.87
12.26
15.0
2.66
0.40
13.80
17.39
13.40
18.19
20.0
2.55
0.51
18.47
23.06
17.96
24.08
25.0
2.46
0.62
23.15
28.70
22.54
29.93
30.0
2.40
0.72
27.84
34.32
27.12
35.75
35.0
2.34
0.82
32.54
39.92
31.72
41.56
40.0
2.30
0.92
37.25
45.51
36.33
47.35
45.0
2.26
1.01
41.96
51.09
40.94
53.12
50.0
2.22
1.11
46.67
56.66
45.56
58.88
60.0
2.16
1.30
56.11
67.78
54.82
70.37
70.0
2.11
1.48
65.57
78.86
64.09
81.82
80.0
2.07
1.65
75.04
89.93
73.38
93.24
90.0
2.03
1.83
84.51
100.97
82.68
104.63
(1) HCV(%) = Horwitz Coefficients of Variation = 2 (1 -0.5 log (claim %/100))
(2) HSD = Horwitz Standard Deviation = (Claim %) HCV %)/100
(3) “Uniform” samples are homogeneous products which can be analyzed by established procedures. In most cases, validated analytical methods are available for these samples.
(4) “Non-uniform” samples are non-homogeneous samples or products which are difficult to sample or subsample. These products may not be uniformly mixed or packaged and include some special formulations like natural products. These types of samples include fertilizer con- taining pesticides, pesticides in pressurized containers, strips, plastic bands, collars, grain and other carriers. Natural product formulations such as rotenone and pyrethrin are also included in this group. When it is necessary to use methods which are not validated for accuracy, pre- cision, and reproducibility in a specific matrix, the “non-uniform” guidelines may be used for allowed deviations. States may use judgment in placing a sample into the “uniform” or “non-uniform” category.
Historical Note
Former rule IV; Former Section R3-3-04 renumbered and amended as Section R3-3-01 effective January 18, 1978 (Supp. 78-1). Section R3-3-704 renumbered from R3-3-04 (Supp. 91-4). New Section adopted by final rulemaking at 5 A.A.R. 4419, effective